Starch and derived products. Heavy metals content. Part 3: Determination of lead content by atomic absorption spectrometry with electrothermal atomization (ISO 11212-3:1997)
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This part of ISO 11212 specifies a method for the determination of the lead content of starch, including derivatives and by-products, by atomic absorption spectrometry with electrothermal atomization. The number of parameters for the procedure involved in the electrothermal atomization is far larger than in flame atomization; it is thus impossible to propose a comprehensive method likely to ensure the attainment of satisfactory results on all types of apparatus currently available. Each analyst should therefore optimize the conditions of use of his/her own apparatus on the basis of general or particular instructions.
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Sisällysluettelo
Foreword
1 Scope
2 Definition
3 Principle
4 Reagents
5 Apparatus
6 Procedure
6.1 General
6.2 Preparation of test sample
6.3 Digestion
6.4 Blank test
6.5 Electrothermal atomization programme
6.6 Determination of the calibration curve
6.7 Determination
7 Expression of results
8 Precision
8.1 Repeatability
8.2 Reproducibility
9 Test report
Annex A Results of interlaboratory test (informative)