Petroleum and natural gas industries. Completion fluids and materials. Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations (ISO 13503-2:2006)
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ISO 13503-2:2006 provides standard testing procedures for evaluating proppants used in hydraulic fracturing and gravel-packing operations. "Proppants" mentioned henceforth in ISO 13503-2:2006 refer to sand, ceramic media, resin-coated proppants, gravel-packing media and other materials used for hydraulic fracturing and gravel-packing operations. The objective of ISO 13503-2:2006 is to provide a consistent methodology for testing performed on hydraulic fracturing and/or gravel-packing proppants.
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Sisällysluettelo
Foreword
Introduction
1 Scope
2 Normative references
3 Abbreviations
4 Standard proppant sampling procedure
4.1 General
4.2 Particle segregation
4.3 Equipment
4.4 Number of required samples — Bulk
4.5 Sampling —Bulk material
4.6 Sampling — Bagged material
5 Sample handling and storage
5.1 Sample reduction
5.2 Sample splitting
5.3 Sample and record retention and storage
6 Sieve analysis
6.1 Purpose
6.2 Description
6.3 Equipment and materials
6.4 Procedure
6.5 Calculation of the mean diameter, median diameter and standard deviation
6.6 Sieve calibration
7 Proppant sphericity and roundness
7.1 Purpose
7.2 Description
7.3 Apparatus capability
7.4 Procedure
7.5 Alternate method for determining average sphericity and roundness
8 Acid solubility
8.1 Purpose
8.2 Description
8.3 Equipment and materials
8.4 Procedure
9 Turbidity test
9.1 Purpose
9.2 Description
9.3 Equipment and materials
9.4 Equipment calibration
9.5 Procedure
10 Procedures for determining proppant bulk density, apparent density and absolute density
10.1 Purpose
10.2 Description
10.3 Bulk density
10.4 Apparent density
10.5 Absolute density
11 Proppant crush-resistance test
11.1 Purpose
11.2 Description
11.3 Equipment and materials
11.4 Sample preparation
11.5 Crush-resistance procedure
12 Loss on ignition of resin-coated proppant
12.1 Objective
12.2 Apparatus and materials
12.3 Loss-on-ignition procedure for whole-grain proppant
Annex A Formazin solution preparation (informative)