SFS-EN ISO 13500:en

Soveltamisala

Suomenkielistä soveltamisalaa ei ole saatavissa.

ISO 13500:2008 covers physical properties and test procedures for materials manufactured for use in oil- and gas-well drilling fluids. The materials covered are barite, haematite, bentonite, nontreated bentonite, OCMA-grade bentonite, attapulgite, sepiolite, technical-grade low-viscosity carboxymethylcellulose (CMC-LVT), technical-grade high-viscosity carboxymethylcellulose (CMC-HVT), starch, low-viscosity polyanionic cellulose (PAC-LV), high-viscosity polyanionic cellulose (PAC-HV) and drilling-grade Xanthomonas campestris (Xanthan gum).
ISO 13500:2008 is intended for the use of manufacturers of named products.

Tämän julkaisun valmistelusta Suomessa vastaa SFS Suomen Standardit, puh. 09 149 9331.

Sisällysluettelo

Foreword
Introduction
1 Scope
2 Normative references
3 Terms, definitions, symbols and abbreviations

3.1 Terms and definitions
3.2 Symbols and abbreviations

4 Requirements

4.1 Quality control instructions
4.2 Use of test calibration materials in checking testing procedures
4.3 Records retention

5 Calibration

5.1 Coverage
5.2 Equipment requiring calibration
5.3 Calibration intervals

6 Packaged material

6.1 Description
6.2 Apparatus — Pallets
6.3 Apparatus — Bags
6.4 Marking — Pallets
6.5 Marking — Bags
6.6 Pallet covers
6.7 Package mass
6.8 Storage
6.9 Recycling

7 Barite

7.1 Principle
7.2 Reagents and apparatus — Density by Le Chatelier flask
7.3 Procedure — Density by Le Chatelier flask
7.4 Calculation — Density by Le Chatelier flask
7.5 Reagents and apparatus — Water-soluble alkaline earths as calcium
7.6 Procedure — Water-soluble alkaline earth metals as calcium
7.7 Calculation — Water-soluble alkaline earths as calcium
7.8 Reagents and materials — Residue of diameter greater than 75 µm
7.9 Procedure — Residue of diameter greater than 75 µm
7.10 Calculation — Residue of diameter greater than 75 µm
7.11 Reagents and apparatus — Particles less than 6 µm in equivalent spherical diameter by sedimentation method
7.12 Procedure — Particles less than 6 µm in equivalent spherical diameter by sedimentation method
7.13 Calculation — Particles less than 6 µm in equivalent spherical diameter by sedimentation method

8 Haematite (hematite)

8.1 Principle
8.2 Reagent and apparatus — Density by Le Chatelier flask
8.3 Procedure — Density by Le Chatelier flask
8.4 Calculation — Density by Le Chatelier flask
8.5 Reagents and apparatus — Water-soluble alkaline earth metals as calcium
8.6 Procedure — Water-soluble alkaline earth metals as calcium
8.7 Calculation — Water-soluble alkaline earth metals as calcium
8.8 Reagents and apparatus — Residues greater than 75 µm and less than 45 µm
8.9 Procedure — Residues of diameter greater than 75 µm and 45 µm
8.10 Calculation — Residues of diameter greater than 75 µm and 45 µm
8.11 Reagents and apparatus — Particles less than 6 µm in equivalent spherical diameter by the sedimentation method
8.12 Procedure — Particles less than 6 µm in equivalent spherical diameter by the sedimentation method
8.13 Calculation — Particles less than 6 µm in equivalent spherical diameter by the sedimentation method

9 Bentonite

9.1 Principle
9.2 Reagents and apparatus — Suspension properties
9.3 Procedure — Rheology of suspension
9.4 Calculation — Rheology of suspension
9.5 Procedure — Filtrate volume of suspension
9.6 Calculation — Filtrate volume of the suspension
9.7 Reagents and apparatus — Residue of diameter greater than 75 µm
9.8 Procedure — Residue of diameter greater than 75 µm
9.9 Calculation — Residue of diameter greater than 75 µm

10 Non-treated bentonite

10.1 Principle
10.2 Reagents and apparatus — Suspension properties
10.3 Procedure — Rheology of the suspension
10.4 Calculation — Rheology of the suspension
10.5 Procedure — Dispersed plastic viscosity of the suspension
10.6 Procedure — Dispersed filtrate volume of the suspension
10.7 Calculation — Dispersed filtrate volume of the suspension

11 OCMA grade bentonite

11.1 Principle
11.2 Reagents and apparatus — Suspension properties
11.3 Procedure — Rheology of the suspension
11.4 Calculation — Rheology of the suspension
11.5 Procedure — Filtrate volume of the suspension
11.6 Calculation — Filtrate volume of the suspension
11.7 Reagents and apparatus — Residue of diameter greater than 75 µm
11.8 Procedure — Residue of diameter greater than 75 µm
11.9 Calculation — Residue of diameter greater than 75 µm

12 Attapulgite

12.1 Principle
12.2 Reagents and apparatus — Suspension properties
12.3 Procedure — 600 r/min dial reading of the suspension
12.4 Reagent and apparatus — Residue of diameter greater than 75 µm
12.5 Procedure — Residue of diameter greater than 75 µm
12.6 Calculation — Residue of diameter greater than 75 µm
12.7 Reagent and apparatus — Moisture
12.8 Procedure — Moisture
12.9 Calculation — Moisture

13 Sepiolite

13.1 Principle
13.2 Reagents and apparatus — Suspension properties
13.3 Procedure — 600 r/min dial reading of suspension
13.4 Reagents and apparatus — Residue of diameter greater than 75 µm
13.5 Procedure — Residue of diameter greater than 75 µm
13.6 Calculation — Residue of diameter greater than 75 µm
13.7 Reagents and apparatus — Moisture
13.8 Procedure — Moisture
13.9 Calculation — Moisture

14 Technical-grade low-viscosity CMC (CMC-LVT)

14.1 Principle
14.2 Reagents and apparatus — Determination of starch and starch derivatives
14.3 Procedure — Determination of starch and starch derivatives
14.4 Interpretation — Determination of starch and starch derivatives
14.5 Reagents and apparatus — Solution properties of water-soluble polymers
14.6 Procedure — Viscometer reading in deionized water
14.7 Procedure — Filtrate volume of suspension
14.8 Calculation — Filtrate volume of the suspension

15 Technical-grade high-viscosity CMC (CMC-HVT)

15.1 Principle
15.2 Reagents and apparatus — Determination of starch and starch derivatives
15.3 Procedure — Determination of starch and starch derivatives
15.4 Interpretation — Determination of starch and starch derivatives
15.5 Reagents and apparatus — Solution properties of water-soluble polymers
15.6 Procedure — Viscometer reading in deionized water
15.7 Procedure — Viscometer reading in 40 g/l salt water
15.8 Procedure — Viscometer reading in saturated salt water
15.9 Procedure — Filtrate volume of the suspension
15.10 Calculation — Filtrate volume of the suspension

16 Starch

16.1 Principle
16.2 Reagents and apparatus — Suspension properties
16.3 Procedure — Viscometer reading in 40 g/l salt water
16.4 Procedure — Filtrate volume of 40 g/l salt solution
16.5 Calculation — Filtrate volume of the 40 g/l salt solution
16.6 Procedure — Viscometer reading in the saturated salt solution
16.7 Procedure — Filtrate volume of the saturated salt solution
16.8 Calculation — Filtrate volume of the saturated salt solution
16.9 Reagents and apparatus — Residue greater than 2 000 µm
16.10 Procedure — Residue greater than 2 000 µm

17 Low-viscosity polyanionic cellulose (PAC-LV)

17.1 Principle
17.2 Qualitative starch determination in water-soluble polymers
17.3 Moisture content
17.4 Filtrate volume
17.5 Fluid apparent viscosity

18 High-viscosity polyanionic cellulose (PAC-HV)

18.1 Principle
18.2 Qualitative starch determination in water soluble polymers
18.3 Moisture content
18.4 Filtrate volume
18.5 Fluid apparent viscosity

19 Drilling-grade xanthan gum

19.1 Principle
19.2 Qualitative starch determination in xanthan gum
19.3 Qualitative guar determination in xanthan gum
19.4 Moisture content
19.5 Particle size
19.6 Fluid viscosity
19.7 Low-shear-rate viscosity
19.8 Calibration of direct-indicating viscometer

Annex A Mineral impurities in barite (informative)
Annex B Test precision (informative)
Annex C Examples of calculations (informative)

Bibliography

Näytä kaikki

Foreword
Introduction
1 Scope
2 Normative references
3 Terms, definitions, symbols and abbreviations

3.1 Terms and definitions
3.2 Symbols and abbreviations

4 Requirements

4.1 Quality control instructions
4.2 Use of test calibration materials in checking testing procedures
4.3 Records retention

5 Calibration

5.1 Coverage
5.2 Equipment requiring calibration
5.3 Calibration intervals

6 Packaged material

6.1 Description
6.2 Apparatus — Pallets
6.3 Apparatus — Bags
6.4 Marking — Pallets
6.5 Marking — Bags
6.6 Pallet covers
6.7 Package mass
6.8 Storage
6.9 Recycling

7 Barite

7.1 Principle
7.2 Reagents and apparatus — Density by Le Chatelier flask
7.3 Procedure — Density by Le Chatelier flask
7.4 Calculation — Density by Le Chatelier flask
7.5 Reagents and apparatus — Water-soluble alkaline earths as calcium
7.6 Procedure — Water-soluble alkaline earth metals as calcium
7.7 Calculation — Water-soluble alkaline earths as calcium
7.8 Reagents and materials — Residue of diameter greater than 75 µm
7.9 Procedure — Residue of diameter greater than 75 µm
7.10 Calculation — Residue of diameter greater than 75 µm
7.11 Reagents and apparatus — Particles less than 6 µm in equivalent spherical diameter by sedimentation method
7.12 Procedure — Particles less than 6 µm in equivalent spherical diameter by sedimentation method
7.13 Calculation — Particles less than 6 µm in equivalent spherical diameter by sedimentation method

8 Haematite (hematite)

8.1 Principle
8.2 Reagent and apparatus — Density by Le Chatelier flask
8.3 Procedure — Density by Le Chatelier flask
8.4 Calculation — Density by Le Chatelier flask
8.5 Reagents and apparatus — Water-soluble alkaline earth metals as calcium
8.6 Procedure — Water-soluble alkaline earth metals as calcium
8.7 Calculation — Water-soluble alkaline earth metals as calcium
8.8 Reagents and apparatus — Residues greater than 75 µm and less than 45 µm
8.9 Procedure — Residues of diameter greater than 75 µm and 45 µm
8.10 Calculation — Residues of diameter greater than 75 µm and 45 µm
8.11 Reagents and apparatus — Particles less than 6 µm in equivalent spherical diameter by the sedimentation method
8.12 Procedure — Particles less than 6 µm in equivalent spherical diameter by the sedimentation method
8.13 Calculation — Particles less than 6 µm in equivalent spherical diameter by the sedimentation method

9 Bentonite

9.1 Principle
9.2 Reagents and apparatus — Suspension properties
9.3 Procedure — Rheology of suspension
9.4 Calculation — Rheology of suspension
9.5 Procedure — Filtrate volume of suspension
9.6 Calculation — Filtrate volume of the suspension
9.7 Reagents and apparatus — Residue of diameter greater than 75 µm
9.8 Procedure — Residue of diameter greater than 75 µm
9.9 Calculation — Residue of diameter greater than 75 µm

10 Non-treated bentonite

10.1 Principle
10.2 Reagents and apparatus — Suspension properties
10.3 Procedure — Rheology of the suspension
10.4 Calculation — Rheology of the suspension
10.5 Procedure — Dispersed plastic viscosity of the suspension
10.6 Procedure — Dispersed filtrate volume of the suspension
10.7 Calculation — Dispersed filtrate volume of the suspension

11 OCMA grade bentonite

11.1 Principle
11.2 Reagents and apparatus — Suspension properties
11.3 Procedure — Rheology of the suspension
11.4 Calculation — Rheology of the suspension
11.5 Procedure — Filtrate volume of the suspension
11.6 Calculation — Filtrate volume of the suspension
11.7 Reagents and apparatus — Residue of diameter greater than 75 µm
11.8 Procedure — Residue of diameter greater than 75 µm
11.9 Calculation — Residue of diameter greater than 75 µm

12 Attapulgite

12.1 Principle
12.2 Reagents and apparatus — Suspension properties
12.3 Procedure — 600 r/min dial reading of the suspension
12.4 Reagent and apparatus — Residue of diameter greater than 75 µm
12.5 Procedure — Residue of diameter greater than 75 µm
12.6 Calculation — Residue of diameter greater than 75 µm
12.7 Reagent and apparatus — Moisture
12.8 Procedure — Moisture
12.9 Calculation — Moisture

13 Sepiolite

13.1 Principle
13.2 Reagents and apparatus — Suspension properties
13.3 Procedure — 600 r/min dial reading of suspension
13.4 Reagents and apparatus — Residue of diameter greater than 75 µm
13.5 Procedure — Residue of diameter greater than 75 µm
13.6 Calculation — Residue of diameter greater than 75 µm
13.7 Reagents and apparatus — Moisture
13.8 Procedure — Moisture
13.9 Calculation — Moisture

14 Technical-grade low-viscosity CMC (CMC-LVT)

14.1 Principle
14.2 Reagents and apparatus — Determination of starch and starch derivatives
14.3 Procedure — Determination of starch and starch derivatives
14.4 Interpretation — Determination of starch and starch derivatives
14.5 Reagents and apparatus — Solution properties of water-soluble polymers
14.6 Procedure — Viscometer reading in deionized water
14.7 Procedure — Filtrate volume of suspension
14.8 Calculation — Filtrate volume of the suspension

15 Technical-grade high-viscosity CMC (CMC-HVT)

15.1 Principle
15.2 Reagents and apparatus — Determination of starch and starch derivatives
15.3 Procedure — Determination of starch and starch derivatives
15.4 Interpretation — Determination of starch and starch derivatives
15.5 Reagents and apparatus — Solution properties of water-soluble polymers
15.6 Procedure — Viscometer reading in deionized water
15.7 Procedure — Viscometer reading in 40 g/l salt water
15.8 Procedure — Viscometer reading in saturated salt water
15.9 Procedure — Filtrate volume of the suspension
15.10 Calculation — Filtrate volume of the suspension

16 Starch

16.1 Principle
16.2 Reagents and apparatus — Suspension properties
16.3 Procedure — Viscometer reading in 40 g/l salt water
16.4 Procedure — Filtrate volume of 40 g/l salt solution
16.5 Calculation — Filtrate volume of the 40 g/l salt solution
16.6 Procedure — Viscometer reading in the saturated salt solution
16.7 Procedure — Filtrate volume of the saturated salt solution
16.8 Calculation — Filtrate volume of the saturated salt solution
16.9 Reagents and apparatus — Residue greater than 2 000 µm
16.10 Procedure — Residue greater than 2 000 µm

17 Low-viscosity polyanionic cellulose (PAC-LV)

17.1 Principle
17.2 Qualitative starch determination in water-soluble polymers
17.3 Moisture content
17.4 Filtrate volume
17.5 Fluid apparent viscosity

18 High-viscosity polyanionic cellulose (PAC-HV)

18.1 Principle
18.2 Qualitative starch determination in water soluble polymers
18.3 Moisture content
18.4 Filtrate volume
18.5 Fluid apparent viscosity

19 Drilling-grade xanthan gum

19.1 Principle
19.2 Qualitative starch determination in xanthan gum
19.3 Qualitative guar determination in xanthan gum
19.4 Moisture content
19.5 Particle size
19.6 Fluid viscosity
19.7 Low-shear-rate viscosity
19.8 Calibration of direct-indicating viscometer

Annex A Mineral impurities in barite (informative)
Annex B Test precision (informative)
Annex C Examples of calculations (informative)

Bibliography

Tuoteryhmä(t)

75.180.10 Tutkimus-, poraus- ja tuotantolaitteet »

Sidokset

Velvoittavat viittaukset

ASTM D 422:1963 Standard Test Method for Particle-Size Analysis of Soils (Withdrawn 2016)
ASTM E 11:2004 Standard Specification for Woven Wire Test Sieve Cloth and Test Sieves
ASTM E 161:2000 Standard Specification for Electroformed Material and Test Sieves

Tekninen komitea

CEN/TC 12 Oil and gas industries including lower carbon energy »

Vahvistuspäivä

22.06.2009

Julkaisupäivä

10.07.2009

Painos

2

Sivumäärä

97

Julkaisun kieli

englanti