Animal feeding stuffs. Determination of nitrogen content and calculation of crude protein content. Part 2: Block digestion and steam distillation method (ISO 5983-2:2009)
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ISO 5983-2:2009 specifies a method for the determination of nitrogen content of animal feeding stuffs according to the Kjeldahl method, and a method for the calculation of the crude protein content. It is suitable for use as a semi-micro rapid routine method using block digestion, copper catalyst, and steam distillation into boric acid. The method is applicable to the determination of greater than 0,5 % mass fraction Kjeldahl nitrogen in animal feeding stuffs, pet foods, and their raw materials. The method does not measure oxidized forms of nitrogen nor heterocyclic nitrogen compounds. The method does not distinguish between protein nitrogen and non-protein nitrogen.
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Sisällysluettelo
Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Sampling
8 Preparation of test sample
9 Procedure
9.1 General
9.2 Test portion
9.3 Determination
9.4 Blank test
9.5 Recovery tests
10 Calculation and expression of results
10.1 Calculation
10.2 Calculation of crude protein content
10.3 Expression of crude protein content results
11 Precision
11.1 Interlaboratory tests
11.2 Repeatability
11.3 Reproducibility
12 Test report
Annex A Results of interlaboratory tests (informative)
Annex B Results of a profiency test; comparison of the colorimetric and potentiometric endpoint determination of the titration (informative)
ISO 1871:1975 Agricultural food products -- General directions for the determination of nitrogen by the Kjeldahl method
ISO 6498:1998 Animal feeding stuffs -- Preparation of test samples
ISO 1871:1975 Agricultural food products -- General directions for the determination of nitrogen by the Kjeldahl method
ISO 6498:1998 Animal feeding stuffs -- Preparation of test samples