ISO 8292-2:2008 specifies an indirect method for the determination of the solid fat content in animal and vegetable fats and oils (hereafter designated "fats") using low-resolution pulsed nuclear magnetic resonance spectrometry. Two alternative thermal pre-treatments are specified: one for general purpose fats not exhibiting pronounced polymorphism and which stabilize mainly in the ß'-polymorph; and one for fats similar to cocoa butter which exhibit pronounced polymorphism and stabilize in the ß-polymorph. Additional thermal pre-treatments, which may be more suitable for specific purposes, are given in an informative annex. The indirect method is less easy to carry out and less reproducible than the direct method, but is more accurate and more universally applicable to all fats.
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Sisällysluettelo
Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviated terms
5 Principle
6 Triolein standard sample
7 Apparatus
7.1 Pulsed nuclear magnetic resonance (NMR) spectrometer, low resolution
7.2 Measurement tubes
7.3 Temperature-maintenance equipment
7.4 Oven, with fan
7.5 Stop-clock
8 Sampling
9 Procedure
9.1 Measurement protocol and test sample
9.2 Oven, water baths and temperature-controlled blocks
9.3 NMR spectrometer
9.4 Filling the measurement tubes
9.5 Removing the thermal history
9.6 Equilibrating at the initial temperature and measuring the 100 % liquid signal
9.7 Crystallization and tempering
9.8 Measuring the SFC
9.9 Number of determinations
9.10 Cleaning the measurement tubes
10 Expression of results
11 Precision
11.1 Interlaboratory test
11.2 Repeatability
11.3 Reproducibility
12 Test report
Annex A Results of interlaboratory tests (informative)
Annex B Theory of indirect method (informative)
Annex C Additional measurement protocols (informative)
ISO 3960:2007 Animal and vegetable fats and oils -- Determination of peroxide value -- Iodometric (visual) endpoint determination
ISO 661:2003 Animal and vegetable fats and oils -- Preparation of test sample
ISO 8292-1:2008 Animal and vegetable fats and oils -- Determination of solid fat content by pulsed NMR -- Part 1: Direct method
ISO 3960:2007 Animal and vegetable fats and oils -- Determination of peroxide value -- Iodometric (visual) endpoint determination
ISO 661:2003 Animal and vegetable fats and oils -- Preparation of test sample
ISO 8292-1:2008 Animal and vegetable fats and oils -- Determination of solid fat content by pulsed NMR -- Part 1: Direct method