Petroleum and natural gas industries. Evaluation and testing of thread compounds for use with casing, tubing, line pipe and drill stem elements (ISO 13678:2010)
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ISO 13678:2010 provides requirements, recommendations and methods for the testing of thread compounds intended for use on threaded casing, tubing, and line pipe connections; and for thread compounds intended for use on rotary shouldered connections. The tests outlined are used to evaluate the critical performance properties and physical and chemical characteristics of thread compounds under laboratory conditions. These test methods are primarily intended for thread compounds formulated with a lubricating base grease and are not applicable to some materials used for lubricating and/or sealing thread connections. It is recognized that many areas can have environmental requirements for products of this type. ISO 13678:2010 does not include requirements for environmental compliance. It is the responsibility of the end user to investigate these requirements and to select, use and dispose of the thread compounds and related waste materials accordingly.
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Sisällysluettelo
Foreword
Introduction
1 Scope
2 Conformance
2.1 Dual citing of normative references
2.2 Units of measurement
3 Normative references
4 Terms and definitions
5 Thread compound characteristics
5.1 Product characteristics
5.2 Physical and chemical characteristics
6 Thread compound performance properties
6.1 Small-scale test
6.2 Frictional properties
6.3 Extreme surface contact pressure (gall resistance) properties for casing, tubing and line pipe
6.4 Fluid sealing properties for casing, tubing and line pipe
7 Quality assurance and control
8 Marking requirements
8.1 Marking
8.2 Labelling
Annex A API modified thread compound (informative)
Annex B Casing, tubing and line pipe reference standard formulation (normative)
Annex C Penetration test (normative)
Annex D Evaporation test (normative)
Annex E Oil separation test (normative)
Annex F Application/adherence test (normative)
Annex G Gas evolution test (normative)
Annex H Water leaching test (normative)
Annex I Frictional properties test (informative)
Annex J Extreme surface contact pressure (galling) test for casing, tubing and line pipe (informative)
Annex K Fluid sealing test for casing, tubing and line pipe (informative)
Annex L Corrosion inhibition tests (informative)
Annex M Compound high-temperature stability test (informative)
ASTM D 217:2010 Standard Test Methods for Cone Penetration of Lubricating Grease
ASTM D 2265:2006 Standard Test Method for Dropping Point of Lubricating Grease Over Wide Temperature Range
ASTM D 4048:2010 Standard Test Method for Detection of Copper Corrosion from Lubricating Grease
ASTM D 217:2010 Standard Test Methods for Cone Penetration of Lubricating Grease
ASTM D 2265:2006 Standard Test Method for Dropping Point of Lubricating Grease Over Wide Temperature Range
ASTM D 4048:2010 Standard Test Method for Detection of Copper Corrosion from Lubricating Grease
ISO 2137:2007 Petroleum products and lubricants -- Determination of cone penetration of lubricating greases and petrolatum