Fine ceramics (advanced ceramics, advanced technical ceramics). Microstructural characterization. Part 2: Determination of phase volume fraction by evaluation of micrographs (ISO 13383-2:2012)
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ISO 13383-2:2012 specifies a manual method of making measurements for the determination of the volume fraction of major phases in fine ceramics (advanced ceramics, advanced technical ceramics) using micrographs of polished and etched sections, overlaying a square grid of lines, and counting the number of intersections lying over each phase. The method applies to ceramics with one or more distinct secondary phases, such as found in Al2O3/ZrO2, Si/SiC, or Al2O3/SiCw. If the test material contains discrete pores, these are to be treated as a secondary phase for the purpose of this method, provided that there is no evidence of grain pluck-out during polishing being confused with genuine pores.
Tämän julkaisun valmistelusta Suomessa vastaa Metalliteollisuuden Standardisointiyhdistys ry, puh. 09 19 231 (vaihde).
Sisällysluettelo
Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Apparatus
4.1 Sectioning equipment
4.2 Mounting equipment
4.3 Grinding and polishing equipment
4.4 Microscope
4.5 Transparent grid
5 Test piece preparation
5.1 Sampling
5.2 Cutting
5.3 Mounting
5.4 Grinding and polishing
5.5 Etching
6 Photomicrography
6.1 General aspects
6.2 Inspection
6.3 Number of micrographs
6.4 Optical microscopy
6.5 Scanning electron microscopy
7 Measurement of micrographs
8 Calculation of results
9 Interferences and uncertainties
10 Test report
Annex A Use of automatic image analysis (AIA) (informative)
Annex B Round-robin verification of this procedure (informative)