Rice. Determination of amylose content. Part 2: Spectrophotometric routine method without defatting procedure and with calibration from rice standards (ISO 6647-2:2020)
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This document specifies two simplified routine methods for the determination of the amylose mass fraction of milled rice, non-parboiled. The main difference between the two methods is the dispersion procedure: method A specifies hot dispersion, and method B specifies cold dispersion. Both methods are applicable to rice with an amylose mass fraction higher than 5 %. NOTE These methods describe simplified procedures for the preparation of samples, which are frequently used in routine laboratories. The methods use the same reagents as the reference method (see ISO 6647-1), but omit the defatting step. Rice samples where the amylose mass fraction has been determined by the reference method are used as standards.
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Sisällysluettelo
Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Sampling
8 Procedure
8.1 Determination of moisture
8.2 Preparation of test sample
8.3 Test portion and preparation of the test solution
8.4 Preparation of the blank solution
8.5 Preparation of the calibration graph
8.6 Determination
9 Expression of results
10 Precision
10.1 Interlaboratory test
10.2 Repeatability
10.3 Reproducibility
11 Test report
Annex A Results of an interlaboratory test for the routine method (informative)
ISO 6647-1:2020 Rice -- Determination of amylose content -- Part 1: Spectrophotometric method with a defatting procedure by methanol and with calibration solutions of potato amylose and waxy rice amylopectin
ISO 712:2009 Cereals and cereal products -- Determination of moisture content -- Reference method
ISO 7301:2011 Rice -- Specification
ISO 6647-1:2020 Rice -- Determination of amylose content -- Part 1: Spectrophotometric method with a defatting procedure by methanol and with calibration solutions of potato amylose and waxy rice amylopectin
ISO 712:2009 Cereals and cereal products -- Determination of moisture content -- Reference method
ISO 7301:2011 Rice -- Specification
ISO 8466-1:1990 Water quality -- Calibration and evaluation of analytical methods and estimation of performance characteristics -- Part 1: Statistical evaluation of the linear calibration function