This document specifies a bending-vibration method based upon resonance curves for determining the flexural complex modulus E*f of homogeneous plastics and the damping properties of laminated plastics intended for acoustic insulation, for example systems consisting of a metal sheet coated with a damping plastic layer, or sandwich systems consisting of two sheet-metal layers with an intermediate plastic layer. For many purposes, it is useful to determine these properties as a function of temperature and frequency.
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Foreword
1 Scope
2 Normative reference
3 Terms and definitions
4 Principle
5 Test apparatus
5.1 General
5.2 Clamps or suspension fibres
5.3 Exciter and detector
5.4 Temperature-controlled enclosure
5.5 Gas supply
5.6 Temperature-measurement device
5.7 Devices for measuring test specimen dimensions
6 Test specimens
6.1 General
6.2 Shape and dimensions
6.3 Preparation
7 Number of test specimens
8 Conditioning
9 Procedure
9.1 Test atmosphere
9.2 Measurement of specimen cross-section
9.3 Measurement of specimen density
9.4 Mounting the test specimens and adjustment of the transducers
9.5 Varying the temperature
9.6 Varying the frequency
9.7 Recording the resonance curve
10 Expression of results
10.1 Symbols
10.2 Calculation of flexural storage modulus, E'f
10.3 Calculation of flexural loss factor, tan δf
10.4 Calculation of flexural loss modulus, E”f
10.5 Plotting the complex modulus as a function of temperature
ISO 1183-1:2019 Plastics -- Methods for determining the density of non-cellular plastics -- Part 1: Immersion method, liquid pycnometer method and titration method
ISO 1183-2:2019 Plastics -- Methods for determining the density of non-cellular plastics -- Part 2: Density gradient column method
ISO 1183-3:1999 Plastics -- Methods for determining the density of non-cellular plastics -- Part 3: Gas pyknometer method
ISO 1183-1:2019 Plastics -- Methods for determining the density of non-cellular plastics -- Part 1: Immersion method, liquid pycnometer method and titration method
ISO 1183-2:2019 Plastics -- Methods for determining the density of non-cellular plastics -- Part 2: Density gradient column method
ISO 1183-3:1999 Plastics -- Methods for determining the density of non-cellular plastics -- Part 3: Gas pyknometer method
ISO 6721-1:2019 Plastics -- Determination of dynamic mechanical properties -- Part 1: General principles